(3) The titration is conducted by running the standard solution from a burette into a known volume of the test solution, which is usually transferred from the stock-bottle to a beaker or basin by means of a pipette.
A standardized solution of ammonium molybdate is then added from a burette.
From the reading of the burette the lead is calculated.
Next 5 cc. of glacial acetic acid are added, the solution cooled, and 5 cc. of a solution of potassium iodide (300 grammes to the litre) and the standard solution of sodium thiosulphate run in from a burette until the brown colour has nearly disappeared.
Without filtering, the standard solution is added from a burette, and from time to time a drop of the solution is removed on the glass stirring-rod and added to a drop or two of a strong solution of uranium nitrate, previously placed on a white porcelain plate.