If an air-tight receptacle is not available, a small percentage of powdered carbon is added to the zinc-dust, to prevent increase in the amount of oxide, which, if present in excess, tends to make the deposit dull.
Thus prepared, the specimens are placed on shelves or movable trays, at intervals of about 6 in., in an air-tight cupboard, on the inner side of the door of which, as a special protection against insects, is suspended a muslin bag containing a piece of camphor.
The mouth of the bottle is then pressed by hand on the peg of the stopper, and the mouth and peg are ground together with a medium of very fine emery and water until an air-tight joint is secured.
Practically any vessel may serve as a receiver - test tube, flask, beaker, &c. If noxious vapours come over, it is necessary to have an air-tight connexion between the condenser and receiver, and to pro vide the latter with an outlet tube leading to an absorption column or other contrivance in which the vapours are taken up. If the substances operated upon decompose when heated in air, as, for example, the zinc alkyls which inflame, the air within the apparatus is replaced by some inert gas, e.g.
The shaft is lined with a cylinder of wrought iron, within which a tubular chamber, provided with doors above and below, known as an P g air-lock, is fitted by a telescopic joint, which is tightly sinkin packed so as to close the top of the shaft air-tight.
